Dafunkphenomena

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I use temperature and freeze acetone.
btcboss2022
i mean that i suppose u are doing alkali-acid extractions , not gassing directly from methanol(or other) after the al/hg amalgam right?
whats the yield of mdma? and final colour?

the glycidate to PMK in large is very easy and just a direct multiplication , but did u tried large scale with the alkali-base-crystallization with good yields?

tnx in advance
 

btcboss2022

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i mean that i suppose u are doing alkali-acid extractions , not gassing directly from methanol(or other) after the al/hg amalgam right?
whats the yield of mdma? and final colour?

the glycidate to PMK in large is very easy and just a direct multiplication , but did u tried large scale with the alkali-base-crystallization with good yields?

tnx in advance
DafunkphenomenaAmalgam? I think you don't read the info of that post.
 

RA!NER

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Hello,

After check and test the methods posted in the thread http://bbzzzsvqcrqtki6umym6itiixfhn...-methyl-pmk-glycidate-conversion-to-pmk.2013/ I decided the post the best method for me:

1. Put 47,5 liters of H2O in the reactor and add 2,5kg of sodium bicarbonate, stirring until complete dissolution, take out the mixture and keep it.
2. Put in the reactor 7L of H2O
3. Add while stirring 1,2kg of sodium hydroxide
4. While the H2O and the sodium hydroxide are mixing and getting temp put 5kG of wax PMK to melt by low heat.
5. When PMK is melted add it to the reactor and put the mixture at 80C reflux during 1 hour stirring.
btcboss2022
Is it possible to carry out the quantities in the same ratio with 1 litre of water etc.? I have calculated everything in smaller quantities in the same ratio.
 

btcboss2022

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Is it possible to carry out the quantities in the same ratio with 1 litre of water etc.? I have calculated everything in smaller quantities in the same ratio.
RA!NERSure.
 

Mr.Blanks00

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hello, sorry if this picture is pmk oil, and what is the cas number for pmk oil.
 

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Mr.Blanks00

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Ok thank,e friend for information.
 

Curiousonion

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How long do the 2 layers take to seperate once it cools down to 25c?
 

Curiousonion

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I thought the original process was from powder form. So it was originally from the oil pmk version that you started not the wax powder? (I tried from the wax powder and once cooled down to room temperature the material does not seperate into 2 layers)
Today I started the process with same PMK cas but in powder form we will see go it goes I will update you if interested.
Thanks.
btcboss2022
 
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