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i assume you are not following the hcl gas route , but im curious, why you cristallize the free-base?
i assume you are not following the hcl gas route , but im curious, why you cristallize the free-base?
To make little mdma crystals, if not you just left with a liquid. You need to make it into shards
i assume you are not following the hcl gas route , but im curious, why you cristallize the free-base?
I use temperature and freeze acetone.
I use temperature and freeze acetone.
For the bicarb wash, do you really need to use 47 liters of water for 5 liters of pmk?
Or do you just wash it enough just to neutralize the acid?
i mean that i suppose u are doing alkali-acid extractions , not gassing directly from methanol(or other) after the al/hg amalgam right?
whats the yield of mdma? and final colour?
the glycidate to PMK in large is very easy and just a direct multiplication , but did u tried large scale with the alkali-base-crystallization with good yields?
tnx in advance
Hello,
After check and test the methods posted in the thread http://bbzzzsvqcrqtki6umym6itiixfhn...-methyl-pmk-glycidate-conversion-to-pmk.2013/ I decided the post the best method for me:
1. Put 47,5 liters of H2O in the reactor and add 2,5kg of sodium bicarbonate, stirring until complete dissolution, take out the mixture and keep it.
2. Put in the reactor 7L of H2O
3. Add while stirring 1,2kg of sodium hydroxide
4. While the H2O and the sodium hydroxide are mixing and getting temp put 5kG of wax PMK to melt by low heat.
5. When PMK is melted add it to the reactor and put the mixture at 80C reflux during 1 hour stirring.
Is it possible to carry out the quantities in the same ratio with 1 litre of water etc.? I have calculated everything in smaller quantities in the same ratio.
hello, sorry if this picture is pmk oil, and what is the cas number for pmk oil.
Amalgam? I think you don't read the info of that post.
of course i did...man im talking about following steps: mdp2p-mdma
Today I started the process with same PMK cas but in powder form we will see go it goes I will update you if interested.
Thanks.
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