Σύνθεση αμφεταμίνης από P2NP μέσω Al/Hg (βίντεο)

[Eddybeaumont]

Bonjours, quelle est la concentration minimum pour acide sulfurique ?

 

[HIGGS BOSSON]

Προκειμένου το άλας να καθιζάνει αμέσως, είναι απαραίτητο να χρησιμοποιηθεί άνυδρο θειικό οξύ και σε διαλύματα με ακετόνη, για παράδειγμα, μπορεί να υπάρχει συγκέντρωση θειικού οξέος 10%

 

[HIGGS BOSSON]

Είτε εξατμίστε ένα υδατικό διάλυμα θειικού οξέος (αποστάξτε το νερό), είτε προσπαθήστε να οξυνίσετε με υδατικό διάλυμα ακολουθούμενο από ψύξη για κρυστάλλωση, 12 ώρες στους +1-2 βαθμούς είναι αρκετές

 

[Kylemalone1297]

How do I test the product to see if it is actualy amphetamine or just white powder that don’t actualy get reacted ?

 

[HIGGS BOSSON]

 

[Kylemalone1297]

Is it supposed to burn into an oil or into a black ash ?

 

[HIGGS BOSSON]

I don't understand your question

 

[Kylemalone1297]

The powder that was produced by amalgam and the one by copper I got won’t burn into an oil when freebased like other amphetamine salts do. So I think it is messed up somehow.

 

[Eddybeaumont]

hello and thank you for this fabulous video. Is it possible to replace mercury (II) nitrate with mercury (II) chloride for amalgamation with aluminum? If so, does the quantity change? if yes in what quantity for the same proportion as in the video please? thank you in advance for your response

 

[G.Patton]

Yes, it's said above and every post about amalgam production. Same molar ration, you need to recount quantity in grams.

 

[golab071]

Would it make sense, when producing larger quantities of the product, to use solvents like DMSO (boiling point: 189°C) or toluene (110°C) instead of IPA (82°C), and to place pieces of broken porcelain in the reactor to stabilize the reaction?

 

[G.Patton]

The reaction is too violate and exothermic. It think, it have no sense.

 

[William Dampier]

DMSO at high temperature and the presence of acid will begin to degrade on DMS and release oxygen as an oxidizing agent. We have a strong release of hydrogen, which in the aggregate can give "explosive gas". Gently with experiments! In addition, DMSO itself is very smelly with high-temperature synthesis in the presence of many components. Try ethylacetate.

 

[michelAMPH]

Ik moet almagaam gaan maken maar nergens geen kwik 2 chloride TE KOOP
WAT kan voor ALMAGAM zorgen

 

[nofuckups]

What's the exact process of making the P2NP+IPA+GAA solution? Is it just mixing the appropriate quantity of each compound in a beaker, stirring it a bit and then letting it cool? I'm not sure why this part was skipped from the video.

 

[G.Patton]

yes, exactly.

 

[William Dampier]

When it has cooled by part of the P2NP can crystallize again. You can add this precipitate to the flask without dissolution or wash off an additional amount of IPA.

 

[nofuckups]

or just warming up the entire solution a bit before pouring into the aluminium amalgam?

 

[romannestor]

Hello
If I've got the aoil premade, what step could I jump into in the process?

 

[G.Patton]

Hi. Jump directly to acidification step 7:24-8:50

 

[romannestor]

Hi! Thanks for your reply!
The problem I've got is that I don't know the measurements.

 

[romannestor]

Got it now! Thanks again!

 

[G.Patton]

You need to reach pH 5.5-6.5 by addition of the acid as it's said in this video or other one (watch Video section).

 

[Eddybeaumont]

please guys, do you have any idea how to get rid of the waste from this synthesis in a "clean" way? thanks in advance

 

[G.Patton]

Hi, look through Laboratory FAQ section. There are several topics dedicated waste and Hg recuperation.

 

[Eddybeaumont]

Thanks mr Patton