JWH-018 synthesis. Small scale.

abbadon

Don't buy from me
Resident
Language
🇺🇸
Joined
May 4, 2022
Messages
51
Reaction score
13
Points
8
out of researches, i know now here it is like this: when recieve a package from abroad, it must have an invoice in spanish, and every post office has an own customs department inside. Packages arrive not at your house they arrive at the post office. you have to be registered there, with phone number and they message you if something arrives. then you have to go there and open it with them together. It was even not easy to find such information.
 

abbadon

Don't buy from me
Resident
Language
🇺🇸
Joined
May 4, 2022
Messages
51
Reaction score
13
Points
8
is it in mexico easy to get the required stuff imported? or maybe in guatemala if someone knows?
 

abbadon

Don't buy from me
Resident
Language
🇺🇸
Joined
May 4, 2022
Messages
51
Reaction score
13
Points
8

i will follow the advice with mexico
 

abbadon

Don't buy from me
Resident
Language
🇺🇸
Joined
May 4, 2022
Messages
51
Reaction score
13
Points
8

hofmaN.

Don't buy from me
New Member
Joined
Jun 28, 2022
Messages
5
Reaction score
0
Points
3
Inhave this , can i use in smal scale ? I have raw materials like for 50g
 

Attachments

  • VDcaSQYhku.jpeg
    VDcaSQYhku.jpeg
    35.8 KB · Views: 345

Paparazzi

Don't buy from me
Member
Language
🇺🇸
Joined
Jul 11, 2022
Messages
3
Reaction score
0
Points
1
Can we use distillation and put hot al2o3 in the way of the solution instead of refluxing?
 

Paparazzi

Don't buy from me
Member
Language
🇺🇸
Joined
Jul 11, 2022
Messages
3
Reaction score
0
Points
1
For all you guys... I've been trying this synthesis for 2 weeks now and nothing.... If there's anyone who's make it please I'm trying to get some help
 

G.Patton

Expert
Joined
Jul 5, 2021
Messages
2,793
Solutions
3
Reaction score
3,060
Points
113
Deals
1
There is manual, what exactly don't you understand?
I don't understand your question. There is two different steps: step 1 with Al2O3 and step 6 with reflux. You have to just repeat manual.
What did you do exactly? Can you explain your procedure step-by-step?
 

D4ftmonk

Don't buy from me
Resident
Joined
Dec 16, 2022
Messages
5
Reaction score
1
Points
3
In step 4, are the sodium and bromopentane mixed in first, or are they mixed into the mixture one by one?

And the step 7, what does it mean that the aluminum oxide is filtered first? Is aluminum mixed into mixtured first or what?

And also during the reflux process, what temperature should we use?

Please explain in more detail step 8.
Help.
 

G.Patton

Expert
Joined
Jul 5, 2021
Messages
2,793
Solutions
3
Reaction score
3,060
Points
113
Deals
1
The sequence is described in step 4. Do it one by one.
What don't you understand? Read about gravity filtration here.
Add 10 ml of water to the reaction vial, place reaction mixture into a freezer and crystalline JWH-018 is formed. Product is filtered on a Schott funnel and Buchner flask.
Suction (vacuum) filtration

You have to click links and read by yourself. Lab FAQ section consist of wide detailed explanations for all necessary procedures.
 

D4ftmonk

Don't buy from me
Resident
Joined
Dec 16, 2022
Messages
5
Reaction score
1
Points
3
Okey, thanks sir. But, what about the temperature when the reflux proses?
 

Eskobar

Don't buy from me
Member
Joined
Dec 19, 2022
Messages
4
Reaction score
0
Points
1
Hi. say when the reaction in the microwave emits yellow smoke. this is normal?
 

G.Patton

Expert
Joined
Jul 5, 2021
Messages
2,793
Solutions
3
Reaction score
3,060
Points
113
Deals
1
Temperature of reflux means temperature when the solution is boiled. You can check solvent boiling point. Do you understand?
 

G.Patton

Expert
Joined
Jul 5, 2021
Messages
2,793
Solutions
3
Reaction score
3,060
Points
113
Deals
1
A little or a lot?
 

Eskobar

Don't buy from me
Member
Joined
Dec 19, 2022
Messages
4
Reaction score
0
Points
1
a lot of. and the material is black
 

G.Patton

Expert
Joined
Jul 5, 2021
Messages
2,793
Solutions
3
Reaction score
3,060
Points
113
Deals
1
Probably, you've burned your synthesis :(
 

Eskobar

Don't buy from me
Member
Joined
Dec 19, 2022
Messages
4
Reaction score
0
Points
1
tell me please. if you increase the dosage of ingredients 10 times. ethanol also ten times?
 

Eskobar

Don't buy from me
Member
Joined
Dec 19, 2022
Messages
4
Reaction score
0
Points
1
I think so too. I will stay more 😉
 

G.Patton

Expert
Joined
Jul 5, 2021
Messages
2,793
Solutions
3
Reaction score
3,060
Points
113
Deals
1
X5 would be enough
 
Top