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Part 3. Making Methamphetamine with Uncle Fester (Video)

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Phenyl-2-propanone (P2P) synthesis from acetone and benzene. Video manual.

Amphetamine synthesis from P2NP via Al/Hg (video)

Phenyl-2-propanone (P2P) synthesis from acetone and benzene. Video manual.

G.Patton
May 28, 2022
Tags

1-phenylpropan-2-one cas 103-79-7 p2p p2p synthesis video phenyl-2-propanone from acetone and benzene phenyl-2-propanone synthesis phenyl-2-propanone synthesis video manual phenylacetone phenylacetone synthesis video manual

Reactions: handle, Looooow, bblanco and 3 others

Very good video. I rather like the videos with text than this voice ( little bit confusing ). But hands down for this video. Thanks

Can we please have a list of the reagents and glassware used in this video, thanks!

1 bromoacetone

Glassware

1. Graduated cylinder
2. 500 ml beaker
3. 500 ml separating funnel
4. Glass tube and air line with pump set to blow
5. Small Erlenmeyer flask (50ml)

Chemicals
1. 25ml Acetone
2. 10g NaOh and H2O to equal 250ml
3. 33ml of bromine in Dcm@ 0.8g/ml
4. 15g sodium carbonate+50ml H20
5. Calcium carbonate to dry bromoacetone

Phenyl acetone
Glassware
1. 250ml round bottom flask set up for heat/stir
2. Pressure equalizing addition funnel (or analogous assembly of glassware)
3. 500ml beaker
4. 500 separating funnel
5. Complete steam and vacuum distillation kit
Chemicals
1. 50 ml benzene
2. 25g Aluminum chloride
3 NaOh solution for cleaning
4. 5ml Hydrochloric acid in 60g ice
5. 5ml NaHo in 60g ice
(Optional 10ml benzene to extract Aquos phase)
6. 4g sodium hydroxide (NaOh) in 60ml water
7. More benzene and water undetermined amount

@aaronsteve

I did this for my own notes. A damn shame it worked poorly. I'm going to attempt to scrutinize it. I suspect that the steam distillation tainted it and it seems unnecessary anyway

Frit Buchner said:
@aaronsteve

I did this for my own notes. A damn shame it worked poorly. I'm going to attempt to scrutinize it. I suspect that the steam distillation tainted it and it seems unnecessary anyway

Did you figure out the issue? If so, what was it?

JankyCoyote said:
Did you figure out the issue? If so, what was it?

Fuck I forgot try, but the radical reactant that turns L meth into D is AIBN

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