Sinteza amfetamina iz P2NP prek Al/Hg (video)

Eddybeaumont

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Bonjours, quelle est la concentration minimum pour acide sulfurique ?
 

HIGGS BOSSON

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In order for the salt to immediately precipitate, it is necessary to use anhydrous sulfuric acid, and in solutions with acetone, for example, there can be a 10% concentration of sulfuric acid
 

HIGGS BOSSON

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Vodno raztopino žveplove kisline bodisi uparite (vodo destilirajte) bodisi poskusite zakisati z vodno raztopino, čemur sledi hlajenje za kristalizacijo, 12 ur pri +1-2 stopinjah je dovolj.
 
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Ali naj bi zgorelo v olje ali v črn pepel ?
 

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Ne razumem vašega vprašanja
 
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Prah, ki je bil proizveden z amalgamom, in tisti z bakrom, ki sem ga dobil, se pri prosti uporabi ne zažgeta v olje, kot se zažgejo druge amfetaminske soli. Zato mislim, da je nekako zmešan.
 

Eddybeaumont

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Pozdravljeni in zahvaljujemo se vam za ta čudoviti videoposnetek. Ali je mogoče živosrebrov (II) nitrat nadomestiti z živosrebrovim (II) kloridom za amalgamacijo z aluminijem? Če da, ali se količina spremeni? če da, v kakšni količini za enak delež kot v videoposnetku, prosim? vnaprej se zahvaljujem za vaš odgovor.
 

G.Patton

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Yes, it's said above and every post about amalgam production. Same molar ration, you need to recount quantity in grams.
 

golab071

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Ali bi bilo pri proizvodnji večjih količin izdelka smiselno namesto IPA (82 °C) uporabiti topila, kot sta DMSO (vrelišče: 189 °C) ali toluen (110 °C), in v reaktor namestiti koščke razbitega porcelana za stabilizacijo reakcije?
 

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The reaction is too violate and exothermic. It think, it have no sense.
 

William Dampier

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DMSO at high temperature and the presence of acid will begin to degrade on DMS and release oxygen as an oxidizing agent. We have a strong release of hydrogen, which in the aggregate can give "explosive gas". Gently with experiments! In addition, DMSO itself is very smelly with high-temperature synthesis in the presence of many components. Try ethylacetate.
 

michelAMPH

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Izdelati moram almagame, vendar nikjer ni na voljo živosrebrovega 2 klorida ZA PRODAJO
KAJ lahko naredi ALMAGAM
 

nofuckups

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Kakšen je natančen postopek izdelave raztopine P2NP+IPA+GAA? Ali je to samo mešanje ustrezne količine vsake spojine v čaši, rahlo mešanje in nato ohlajanje? Ne vem, zakaj je bil ta del v videoposnetku izpuščen.
 

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yes, exactly.
 

William Dampier

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When it has cooled by part of the P2NP can crystallize again. You can add this precipitate to the flask without dissolution or wash off an additional amount of IPA.
 

romannestor

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Pozdravljeni
Če imam vnaprej pripravljeno olje, v kateri korak v postopku bi lahko skočil?
 

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Pozdravljeni. skočite neposredno na korak kisanja 7:24-8:50
 
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G.Patton

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Z dodajanjem kisline morate doseči pH 5,5-6,5, kot je navedeno v tem ali drugem videoposnetku (oglejte si razdelek Video).
 

Eddybeaumont

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prosim, fantje, ali imate kakšno idejo, kako se na "čist" način znebiti odpadkov iz te sinteze? vnaprej hvala.
 

G.Patton

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Pozdravljeni, preglejte razdelek Pogosta vprašanja in odgovori v laboratoriju. Tam je več tem, ki so posvečene odpadkom in rekuperaciji Hg.
 
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