Amphetamine synthesis from P2NP via Al/Hg (video)

[UWe9o12jkied91d]

Cam somebody in great detail describe to me the exact moment I should pour off the mercuric solution from the aluminum when preparing an aluminum amalgam? It is unclear if there needs to be a heavy gray thick precipitate or not.

JackIf your precipitate is thick and the mass has turned an opaque light gray you are way past your point.If most of your aluminium sinks ay first a good indication is when most of it floats to the top.Also make sure youre using enough salt for the amount of Al, too little and amalgamation itself is too violent, turns white, bubbles like crazy etc.

 

[Jack]

If I add the reaction mixture and no reaction begins, I must heat it to start it yes?

 

[UWe9o12jkied91d]

You mean adding salt to aluminium? It should be a reaction but very gentle, I head using 0.1 / 10-12g Al is best.After adding mercuric salt swil amd observe , no need to heat.
If you mean adding p2np sol over amalgam then most likely your amalgam is incorrect.

 

[andre010]

Hello again, I found a vendor for Mercury Nitrate, it is cas: 7783-34-8 Mercury (II) nitrate Monohydrate !

Is this the correct Mercury Nitrate ?

btw. many thanks for your work and your help here !

 

[andre010]

Hello again, I found a vendor for Mercury Nitrate, it is cas: 7783-34-8 Mercury (II) nitrate Monohydrate !

Is this the correct Mercury Nitrate ?

btw. many thanks for your work and your help here !

andre010Found the answer myself, thank you anyway...

the recherche for my book is complete now ;-)

 

[Jack]

Can anybody tell me how important to the reaction proceeding is the presence of water in the reaction mixture?

 

[lemon]

Can aluminium foil with a thickness of 0,018mm be used? From a well-known chemical manufacturer

And regarding the acetic acid, I can get technical grade 80% and food grade 80%, which is the better option?

Thanks

 

[G.Patton]

Can anybody tell me how important to the reaction proceeding is the presence of water in the reaction mixture?

JackIt is necessary to produce hydrogen H2 gas. You can read about reaction in this topic.

And regarding the acetic acid, I can get technical grade 80% and food grade 80%, which is the better option?

You can. It's better to use food grade.

 

[lemon]

Is the condenser only needed for health reasons due to the vapor?

If I'm outside can I work without condenser? Wouldn't have some big losses?

 

[G.Patton]

Is the condenser only needed for health reasons due to the vapor?

If I'm outside can I work without condenser? Wouldn't have some big losses?

lemonWith all my respect to beginners, you can open comment section and read. This question is already discussed here.

 

[the money]

welcome everybody
I want to share with you my experiences, I tried to cook amphetamine
, I failed in the first experiment
and I failed in the second experiment
, but I succeeded in the third experiment

My third experience was like this

I added 12 grams of aluminum in a 3 liter beaker and added to it 4 ml of mercury nitrate and one liter of distilled water and left it to react for ten minutes
, after which I removed the contaminated water,
then cleaned it with two parts of water
....
Next, I added a solution of isopropyl alcohol, acetic acid, and p2np,
and after that the temperature went up,
I cooled it down a bit and left it to react for about 30 minutes

.....
Then I dumped it into a container and added a sodium hydroxide solution to 11 ph

....
After that, amphetamine oil was extracted

.....
Then add acetone with sulfuric acid to drip amphetamine oil to pH 6

....
8 grams of amphetamine were obtained

....

Special thanks to teacher
G.patton
for helping me

 

[InLikeFlynn]

welcome everybody
I want to share with you my experiences, I tried to cook amphetamine
, I failed in the first experiment
and I failed in the second experiment
, but I succeeded in the third experiment

My third experience was like this

I added 12 grams of aluminum in a 3 liter beaker and added to it 4 ml of mercury nitrate and one liter of distilled water and left it to react for ten minutes
, after which I removed the contaminated water,
then cleaned it with two parts of water
....
Next, I added a solution of isopropyl alcohol, acetic acid, and p2np,
and after that the temperature went up,
I cooled it down a bit and left it to react for about 30 minutes

View attachment 8171
.....
Then I dumped it into a container and added a sodium hydroxide solution to 11 ph
View attachment 8172
View attachment 8173
View attachment 8174
....
After that, amphetamine oil was extracted

View attachment 8175
.....
Then add acetone with sulfuric acid to drip amphetamine oil to pH 6

View attachment 8177
....
8 grams of amphetamine were obtained

View attachment 8178


....

Special thanks to teacher
G.patton
for helping me

ForyouWhat did you do different from the 1st and 2nd attempts to gave success on the 3rd attempt?

 

[UWe9o12jkied91d]

welcome everybody
I want to share with you my experiences, I tried to cook amphetamine
, I failed in the first experiment
and I failed in the second experiment
, but I succeeded in the third experiment

My third experience was like this

I added 12 grams of aluminum in a 3 liter beaker and added to it 4 ml of mercury nitrate and one liter of distilled water and left it to react for ten minutes
, after which I removed the contaminated water,
then cleaned it with two parts of water
....
Next, I added a solution of isopropyl alcohol, acetic acid, and p2np,
and after that the temperature went up,
I cooled it down a bit and left it to react for about 30 minutes

View attachment 8171
.....
Then I dumped it into a container and added a sodium hydroxide solution to 11 ph
View attachment 8172
View attachment 8173
View attachment 8174
....
After that, amphetamine oil was extracted

View attachment 8175
.....
Then add acetone with sulfuric acid to drip amphetamine oil to pH 6

View attachment 8177
....
8 grams of amphetamine were obtained

View attachment 8178


....

Special thanks to teacher
G.patton
for helping me

ForyouNice, grats

 

[nkd23]

Hi
I have problems to get H2SO4 conc in Europe/AT

H2SO4 15% is the strongest I'm able to get
Is it possible to produce with 15% ?

 

[Gale]

Amalgamation problems,

My solvent temp is around 0c starting and when I add merc to aluminum it takes forever to start and I've ruined some product adding it to soon. Seems like it will take like 3 hours in this temp. Am i right? I lost my shit at the lab I was really upset waiting there so late after I finally sourced some ultra pure Ai I thought it would speed things up, it was getting dull, but I had to leave at that point and I was so upset.

My ai is like .06 I think it was cut like nails, not how I asked and wanted so I decided to take initiative and cut it with scissors I got blisters lol

 

[hjames]

Is it better thicker or thinner alu foil?
I can obtain 9,10,11,12 microns thickness

 

[the money]

I used regular kitchen aluminum foil that you can get from any store

 

[Jack]

Can the acetic acid be replaced with formic acid?

 

[G.Patton]

Can the acetic acid be replaced with formic acid?

JackYou can don't use acid at all. I told about in in this topic.

 

[hjames]

If I understood correctly in one video freebase is mixed with acetone 1:1 and used only Sulfuric acid, and in another video sulfuric acid is used diluted with acetone
What is better? What is an advantage if freebase is mixed 1:1 with acetone?

 

[G.Patton]

What is better? What is an advantage if freebase is mixed 1:1 with acetone?

hjamesThere is no difference.