Faster way to make crystals
G.Patton
Hello, depends on what do you need (large crystals or small ones)
Hello, depends on what do you need (large crystals or small ones)
Faster way to make crystals
4mmc 100g
woda 200ml
aceton 50ml
witamina c 3g
heat the water to 60 ° add 4mmc, stir until it dissolves, add acetone and add vitamine c keep the temperature at 60 °. Pour the solution into a bowl, can be glass or plastic, and in a few days at 22 ° -25 ° you will get a crystal in the form of sticks. thank you so much for your attention
1 give 1 ml water for 1 g powder cook and let closed in coolbox when I open is nothing crystalize after 1 day.
This must be open or closed and wait which method is good
4-Methylmethcathinone crystallization conditions:
- Constant temperature 22-24 ºC;- Dry air (<40% relative humidity);
- Container volume;
Simple method
Isopropyl alcohol (IPA) or ethanol solution with water is prepared in ratio 30/70, 50/50, 70/30. Proportions are adjusted according with a tasks and a crystallization container volume. Time of crystallization and crystal size depend on amount of water in solution. The more water, the bigger the crystals and longer crystallization procedure. Average proportion of mephedrone hydrochloride to water is 1 g per 2-3 ml of solvent. The solution is heated to a light boiling (small bubbles). Then mephedrone hydrochloride is added in portions so that it has time to dissolve. Next, the product is dissolved, boil for a couple minutes and the solution is poured into a crystallization dish. Plastic and glass dishes are mostly used. The solution layer with height 1-2 cm height gives a fraction with a sugar crystals size. The solution layer 3-5 cm height gives an up to 5 mm fraction. Air-conditioned boxes, fume hoods and air dryers can be used for this procedure. Wet crystals are obtained after solvent evaporation, which are well dried under dry air flow, infrared radiation (IR lamp or IR heater) or in a vacuum desiccator.
Gradual cooling method View attachment 437
Сrystallization centers are formed in the solution, when solution is evaporated for 50% or more. To accelerate the crystallization process, the mixture is gradually cooled. A crystallization dish is placed into a refrigerator (4 ºC) for 8-12 h, then it is moved into a freezer (-17-20 ºC) for 8-12 h.
Rotary evaporator crystallization technique (fine fraction)
Mephedrone hydrochloride is dissolved in a solvent in the proportion of 1 g per 1 ml. The solution is placed in the rotary evaporator flask and distilled. The deeper vacuum, the lower the boiling point of the solution. Large amount of fine crystals are obtained by this way.
It is possible to evaporate the solution with a hot air fan from a crystallization dish in the rotary evaporator absence case. In this case, glass or ceramic heat-resistant glassware is used. It is important to prevent overheating of the product and, as a result, its deterioration.
Crystallization technique with rapid cooling
Mephedrone salt is dissolved in hot water in the proportion 1 g per 1 ml in a boiling hot water. Ethanol 0.5 l or other polar organic solvent is added after complete dissolving. The hot solution is poured into a plastic containers to fill ½ or 2/3 volume, sealed and cooled in a freezer at -17-20 ºC. There is a chance that the product will not precipitate out. In this case crystals are filtered and the solution is additionally evaporated.
Сrystallization method in brine solution
Sodium chloride (NaCl) 23 g is dissolved in distilled water (H2O) 100 ml. Mephedrone hydrochloride 100 g is dissolved in this brine solution, the solution should be heated for better solubility. The solution is poured into a plastic container to fill ½ or 2/3 volume and sealed tightly. Crystals are grown at low temperature -18 ºC. If the temperature is cooled below -18 ºC, the brine solution is frozen.
Tell me about crystallization in brine, how to separate sodium chloride or calcium chloride from Mephedron? There is no information about this in your main post.
Why do you need to use this strange method? It looks dirty and ineffective. Probably I can help you with an advice? What do you want to do?
Can you tell you something proven and effective?
There are several method with clear explanation. Do you need something else?Сrystallization method in brine solution
Sodium chloride (NaCl) 23 g is dissolved in distilled water (H2O) 100 ml. Mephedrone hydrochloride 100 g is dissolved in this brine solution, the solution should be heated for better solubility. The solution is poured into a plastic container to fill ½ or 2/3 volume and sealed tightly. Crystals are grown at low temperature -18 ºC. If the temperature is cooled below -18 ºC, the brine solution is frozen.
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here is a photo of the crystals at that link.
and this is another method. dissolve 4-mmc in vodka 1g per 2.5ml. and forget about the solution for 4-5 weeks at room temperature. vodka evaporates, crystals remain in the container
minus temperature is not a prerequisite. you can do the same at a temperature of + 20C. but the higher the temperature in the room, the more 4-mmc will remain in the mother liquor. at -8C almost all 4-mmc will fall out of solution. at + 20C about 70% will fall out, about 30% will remain in the water. but what prevents you from driving off the water and getting the remains of 4-mmc, and then repeating the crystallization process again?
and this is another method. dissolve 4-mmc in vodka 1g per 2.5ml. and forget about the solution for 4-5 weeks at room temperature. vodka evaporates, crystals remain in the container
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