Question Need help in 4mmc synthesis step

[Kiteretsu_D]

So i first added 2b4mp then bezen in flask then i added methylamine 40% and started stiring with megnetic stirrer, now i don't have heat source so how long should i stirrer for without heat? And how will i know the reaction is done? At starting the liquid was white right now its turned greenish colour

 

[Argento]

why did you use benzene instead of ethyl acetate or DCM?

 

[The-Hive]

Read this thread

 

[Osmosis Vanderwaal]

Its all a blur, but i seem to recall refluxing at under 105c for 2 hours or something. im not confident it will even react without the application of heat. Im old and all of the synths in my head turn into one massive synthesis of an end-game drug, and its hard to remimber which procedure goesvwith which synth, so i might be mistaken but i think you need at least enough energy to kick off the reaction

 

[Berlin777]

You can do cold synthesis and stir for 16h at room temperature