MDMA/ecstasy saflaştırma yöntemi

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Merhaba arkadaşlar, katkı için teşekkürler, çok iyi çalışıyor ama bir şüphem var, kristalleştirirken (kristaller çok iyi çökeliyor) tipik mdma kristalleri gibi kristaller elde etmiyorum, daha çok kar tanelerine benzer bir şey, karlı bir günde bir bardakta buz kırılmasına, cam ama çok kırılgan. Neden sağlam bir cam elde edemiyorum? Teşekkür ederim ve selamlar 😊
 

G.Patton

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Merhaba, rica ederim! Kristalizasyon prosedürü için buzdolabı kullanıyor musunuz? Ne kadar hızlı soğursa kristaller o kadar küçük olur.
 
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Evet, tabii ki, önce oda sıcaklığına gelene kadar dışarıda bırakıyorum, sonra %15 veya 20'si kristalleşti, sonra 2 saat buzdolabına ve sonra 3 saat dondurucuya koyuyorum. Yıkanan ürünün neredeyse %100'ü kristalleşiyor, ancak kristaller çok kırılgan, paketleme için kullanıldığında kuma dönüşüyorlar
 

Mr Good Cat

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Birkaç kez IPA yaptım ve sanırım bu "kum" kristal tarzı IPA kristalizasyonunun doğal bir özelliği. Büyük kaya kristalleri elde etmek için suda yeniden kristalleştirmeyi deneyin.
 
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Mr Good Cat

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Fark ettiğim şey, IPA, sentezin yan ürünü olan yapışkan siyah bileşiği çıkarmak için iyidir.
 

William Dampier

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Large crystals are obtained with the inclusion of a water molecule. Therefore, sometimes it is better to use aq. HCl acid or add water additionally. You must begin crystallization at room temperature so that the process does not begin quickly. If you show a photo of your crystals, maybe I will tell you that you can change for this and get it in a larger size.
 

Keychainsaw

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I read heat makes it brown in here,
I had some issues with the hobby project. The sirup smelled like methylamine in the glass tray and im afraid there might be some methylamine hcl in the end product. Either way this looks fucked up and it looks like it doesnt want to dry any further. Acetone wash just usually turns it into a black tar. Have to say i forgot to dry it does the 4% aq make a bid difference?

This is what i managed to scrape together and kind of dry out. It tastes more salty than bitter. I dont know how methylamine hcl tastes but drying in the oven doesn't make it appear dryer. Its more tarlike than anything else. I'm ready to give up and just flush it. I did manage to get a whiter one with acetone wash but it has the same non bitter taste. Slightly salty. Could other salts have formed in the process? Maybe the aq layer was pipetted up aswell, in that case it might contain trace amounts of mercury?
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G.Patton

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Have you dried this in an oven? At what temp? I assume, there are not a lot of MDMA in this "product".
Looks looks dog shit.
 

Keychainsaw

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105 Celcius. I did manage to get a few gr of good stuff out it before with acetone washes it yielded only a few gr. Thanks for confirming to toss it than i stop wasting and experimenting on it. To be honest the taste test did not pass and it tasted salty and slightly metallic. It didnt want to dry or crash i will simply dump it. Thanks for the fast reply.
 
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