has anyone tried the Al/Hg amalgam method in small quantities?
i have tried it with the same ratio but 10 times less from everything and got greenish/grey precipitate instantly after pouring p2np solution onto the amalgam
any idea what might happened?
Are you sure in your P2NP quality? Have you recrystallized this precursor and check melting point?
Are you sure in your P2NP quality? Have you recrystallized this precursor and check melting point?
i think he meant the amalgamation was not good enough for the reaction.
Which might be the case, I could not nail it the yet, complications happened in the past with amalgamation. Last time I tried it the foil started crackling and smoking after being rinsed, but this time it wasnt reacting as aggressively, maybe that was the problem.
I got the P2NP from a vendor advertised here on the forum with good reviews, so I would say quality is good, will recrystallize and check melting point in near future.
Hello, does anyone know of any European supplier of mercuric nitrate, mercuric chloride or nitric acid? A week ago I bought nitric acid from a supplier mentioned in this thread http://www.aurelio-online.com/
but I don't know if they will send it to me.
Thanks!
Hello, does anyone know of any European supplier of mercuric nitrate, mercuric chloride or nitric acid? A week ago I bought nitric acid from a supplier mentioned in this thread http://www.aurelio-online.com/
but I don't know if they will send it to me.
Thanks!
Hello, does anyone know of any European supplier of mercuric nitrate, mercuric chloride or nitric acid? A week ago I bought nitric acid from a supplier mentioned in this thread http://www.aurelio-online.com/
but I don't know if they will send it to me.
Thanks!
Greetings to everyone again, we have a few questions about synthesis
1. Is it possible for P2NP to spoil or lose its property?
2. How to recognize the corrupt P2NP?
3. How and in what conditions do you keep P2NP? Should he be in the cold?
4. During synthesis, in the first step Al Amalgam. We worked on the instruction and 4 times the amalgation failed. When we added "Our Made Living Nitrate" reaction was too fast, in just ten minutes bubbles were created, dark liquid and all aluminum rose to the surface and we decided to assess amalgation and there were very few other aluminums, we have the impression that it has melted during amalgation. And when we added a solution of the prepared P2NP, the reaction was missing and there was no. What went wrong?
5. Before the unsuccessful synthesis above, we had one that had a great course, but at the end, when adding a caustic soda solution, we got too much of an amphetamine base, about 100ml, while in earlier procedures we got similar to the video synthesis. We realized that something was wrong and we added sulfuric acid as well, but it didn't respond.
6. Can it be used in the last step, instead of acetone, isopropile alcohol with sulfuric acid? Or was it exclusively acetone?
7. On one occasion we had an unusual large yield where we had approximately 3x more paste obtained. We mean a wet paste, once squeezed through the fabric. What could have been the cause?
P2np stood for a long time because we couldn't get to the mercury, so we doubt that our P2NP broke down, so we asked those few questions.
Otherwise we had a dozen successful synthesis until then.
Thanks for the answers in advance
Congratulation! It would be nice. Share us your result please.
How to recognize the corrupt P2NP?
yes, i willi try.
my english is very poor, soit might take a while to answer
first i want to ask about P2PN
where can i find a trusted seller?
(dont know if can i do this question here, if i cant, tell me to erase it please)
Our team brings together the best specialists from different fields.
We are ready to share our experience, discuss difficult issues and find new solutions.
Connect notifications to always stay in touch with the forum!
The BB Forum team is looking for cooperation: