Amphetamine synthesis from P2NP via Al/Hg (video)

[user123qwe]

I have a question. Are these crystals that appear in the bottom gray layer of the base solution P2NP that has not reacted? It is curious, they have appeared just the time I have had the active reaction for about two hours, longer than usual. (I usually allow half an hour to pass before proceeding with the basification)

The resulting yield has been very high (75%, more or less), and I think the final appearance is quite satisfactory.

 

[Acidosis]

I have a question. Are these crystals that appear in the bottom gray layer of the base solution P2NP that has not reacted? It is curious, they have appeared just the time I have had the active reaction for about two hours, longer than usual. (I usually allow half an hour to pass before proceeding with the basification)
View attachment 7771
The resulting yield has been very high (75%, more or less), and I think the final appearance is quite satisfactory.
View attachment 7772

user123qwehello friend... yes, as our friend Gpatton says, those crystals are salts, in this case they are sodium salts that are formed in the mud layer when it has been at high temperatures and then there has been a rapid drop in temperature, you see, it is normal see them when you meet those conditions that you explain. For the rest the result looks good... health and joy brother!.

 

[user123qwe]

hello friend... yes, as our friend Gpatton says, those crystals are salts, in this case they are sodium salts that are formed in the mud layer when it has been at high temperatures and then there has been a rapid drop in temperature, you see, it is normal see them when you meet those conditions that you explain. For the rest the result looks good... health and joy brother!.

AcidosisThanks for your answer! Lately I have focus my TEK taking care of the temperature, trying to never reach 60-65ºC. And it has been a game changer. The yields and the quality has improved significantly.

 

[spikkel]

I got to know this forum through @HIGGS BOSSON YouTube channel and I must say you are a true example of how it should be. Work safely, pass on knowledge, be prepared to come up with different or newer ways to get to the end product, keep busy and stay safe, I will soon also have some questions about our method of synthesis, thanks in advance

 

[Phanyl666]

Anyone know how to recover the mercury after running a bath, id like to recycle

 

[Phanyl666]

Sorry batch

 

[brendaxs]

Hi guys, where can i buy mercury nitrate. Im in west europe.

Thanks

 

[sevenlakes5577]

well i fiucked up by followin the video. when mixing the P2NP it states 100ml of IPA and 50ml of H20 not GAA, maybe wanna fix that as i guess i just wasted 25g of P2NP. unless there is a remedy for this...

 

[Acidosis]

well i fiucked up by followin the video. when mixing the P2NP it states 100ml of IPA and 50ml of H20 not GAA, maybe wanna fix that as i guess i just wasted 25g of P2NP. unless there is a remedy for this...

sevenlakes5577Hello friend, I assume that when doing the calculations you already added 250ml of ispropyl alcohol and your mistake was using 125ml of water, well, listen to me and now add 50ml more of alcohol and instead of adding 125ml of acetic acid use 200ml and continue your synthesis Normally, that mistake won't ruin your work, just use a drying agent(magnesium sulfate) for your alcohol-free base to dry up any remaining water molecules...ok??..follow these instructions and proceed with peace of mind.

 

[sevenlakes5577]

Hello friend, I assume that when doing the calculations you already added 250ml of ispropyl alcohol and your mistake was using 125ml of water, well, listen to me and now add 50ml more of alcohol and instead of adding 125ml of acetic acid use 200ml and continue your synthesis Normally, that mistake won't ruin your work, just use a drying agent(magnesium sulfate) for your alcohol-free base to dry up any remaining water molecules...ok??..follow these instructions and proceed with peace of mind.

AcidosisWell I had scaled up the reaction by a factor of 2.5 so I added 250 IPA and 150 DI-H20 and then 25g of clean yellow P2NP. Thank you so muchfor replying tho. I had hope someone on here would be able to help me.

 

[firefang]

My solution:

 

[Marvin "Popcorn" Sutton]

My solution:
View attachment 13574

firefangWhat is it?

 

[w2x3f5]

What is it?

Marvin "Popcorn" SuttonAspirin bro)))

 

[firefang]

My solution:
View attachment 13574

firefang...

 

[MrMarvin]

Hello Guys.
Im only able to get 14,9% sulphuric acid in my country.
Is it possible to use it?

 

[UWe9o12jkied91d]

Hello Guys.
Im only able to get 14,9% sulphuric acid in my country.
Is it possible to use it?

MrMarvinNo, but you can boil off the water

 

[MrMarvin]

No, but you can boil off the water

UWe9o12jkied91dThanks for your responding.
How pontet should my sulfuric acid bei?

 

[UWe9o12jkied91d]

Thanks for your responding.
How pontet should my sulfuric acid bei?

MrMarvinAs much as possible, every gram of water is a gram of product lost when precipitating more or less

 

[MrMarvin]

As much as possible, every gram of water is a gram of product lost when precipitating more or less

UWe9o12jkied91dSo i can simply distill the 15% sulfuric acid solution at 100-105°c.
Sulfuric acid's boiling Point ist 337°c

 

[UWe9o12jkied91d]

So i can simply distill the 15% sulfuric acid solution at 100-105°c.
Sulfuric acid's boiling Point ist 337°c

MrMarvinYes, sulphuric acid dosen’t need to come over, youre just trying to lose the water

 

[MrMarvin]

Yes, sulphuric acid dosen’t need to come over, youre just trying to lose the water

UWe9o12jkied91dOkay, thanks.
Do you know how I can check the temperature reliable?

 

[FredDurst]

Okay, thanks.
Do you know how I can check the temperature reliable?

MrMarvinHi MrMarvin, how did you get on with concentrating the sulphuric acid solution?

I have the same problem

 

[MrMarvin]

And how beginner friendly is this Synthesis?
Does Somebody have tips for the beginnin?
Maybe Something that He or she could have done better at the begin...
And another question: how can i Check the Temperature reliable?

 

[MrMarvin]

Thanks for your responding.
How pontet should my sulfuric acid bei?