googie

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Like @Lordoftheshard 2 said use hypophosphoric acid for an easier and quicker method if you can find it.

Forget match strike pads if you can't get red easily, order these. https://www.aliexpress.com/w/wholes...f=auto_suggest&spm=a2g0n.productlist.header.0

Moisten slightly with acetone and let it soak a little, scrape the phosphorus off.

As for HCl generation, be careful with foil it can get violent. Keep going with non iodized salt and adding hydrochloric dropwise in a sealed vessel with a hose out the top. If you don't have lab equipment a plastic coke bottle with a small tube through the lid will do.
 
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zaners

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Like @Lordoftheshard 2 said use hypophosphoric acid for an easier and quicker method if you can find it.

Forget match strike pads if you can't get red easily, order these. https://www.aliexpress.com/w/wholes...f=auto_suggest&spm=a2g0n.productlist.header.0

Moisten slightly with acetone and let it soak a little, scrape the phosphorus off.

As for HCl generation, be careful with foil it can get violent. Keep going with non iodized salt and adding hydrochloric dropwise in a sealed vessel with a hose out the top. If you don't have lab equipment a plastic coke bottle with a small tube through the lid will do.
googieHow do you go about getting the red p off the paper? Can you just scrape it??
 
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SoldadoDeDrogas

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I asked the same ,and it says it under the link
zanersSoak in acetone long enough - about 30 minutes - and it will basically fall off by itself, you may have to rub it a little. You should not have to put in effort to 'scrape' it off. Just wash it and filter to collect clean RP. Then cook RP on low heat in %20 NaOH solution for about an hour. Wash, filter and dry RP. After drying it will be ready to be reacted with I2. If you can get sodium hypophosphite to make your phosphorous acid it is much better for this reaction than RP.
 

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Soak in acetone long enough - about 30 minutes - and it will basically fall off by itself, you may have to rub it a little. You should not have to put in effort to 'scrape' it off. Just wash it and filter to collect clean RP. Then cook RP on low heat in %20 NaOH solution for about an hour. Wash, filter and dry RP. After drying it will be ready to be reacted with I2. If you can get sodium hypophosphite to make your phosphorous acid it is much better for this reaction than RP.
SoldadoDeDrogasThx
 

zaners

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Soak in acetone long enough - about 30 minutes - and it will basically fall off by itself, you may have to rub it a little. You should not have to put in effort to 'scrape' it off. Just wash it and filter to collect clean RP. Then cook RP on low heat in %20 NaOH solution for about an hour. Wash, filter and dry RP. After drying it will be ready to be reacted with I2. If you can get sodium hypophosphite to make your phosphorous acid it is much better for this reaction than RP.
SoldadoDeDrogasIs that what phosphoric acid cleaner is?
 

SoldadoDeDrogas

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Is that what phosphoric acid cleaner is?
zanersThe sodium hypophosphite -> hypophosphorous acid <=> red phosphorous + I2 = Hydriodic acid. It is what Uncle Fester talks about when he goes on about the electroless nickel plating. It is sold as the 'C component'. Or 'R component' for replenisher, I believe. You may be correct I am not sure exactly how you mean. You will have to do a little research or keep asking.
 

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The sodium hypophosphite -> hypophosphorous acid <=> red phosphorous + I2 = Hydriodic acid. It is what Uncle Fester talks about when he goes on about the electroless nickel plating. It is sold as the 'C component'. Or 'R component' for replenisher, I believe. You may be correct I am not sure exactly how you mean. You will have to do a little research or keep asking.
SoldadoDeDrogasThx,I found info
 

EDDYCORONEL

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I HAVE FERNTERMINA, RESEARCHING IT IS VERY SIMILAR TO THE PSEUDO MOLECULE, IT DOES NOT HAVE THE RADICAL OH, I AM NOT A CHEMIST BUT IF I NO LONGER HAVE THE OH, COULD I SKIP THE STEP OF PHOSPHORUS AND IODINE?
 

tankikan

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Any thought on above method?
 

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B.d.p.n.e

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the one in the video is the whole process if I do exactly as in the video it's ok it seems too easy yes I ask?
SupergreenThe methods in the video are correct, but I think the video is fake, some things are not as they should be
 
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alex7736

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If I follow this video as it is and follow the recipe, can I make a synthesis? In the video, he says one and a half hours enough for the reaction to be completed, and he does not use Ruflex . If I do the same thing, can I succeed?
 

Throw-off

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If I follow this video as it is and follow the recipe, can I make a synthesis? In the video, he says one and a half hours enough for the reaction to be completed, and he does not use Ruflex . If I do the same thing, can I succeed?
alex7736Once I was 2hrs into dancing with the flask, and the power went out and fuck me the Susi didn't convert over and it was a shit job the next 48 hrs finding it in the RM mixture, so no if you don't reflux and only mix for 1.5hrs you'll be wasting your time and susi
 

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Has anyone tried or have any information of a Birch Reduction using Microwave irradiation, preferably using a Hypo/I route?
 

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I done the second method of the OTC pill extraction and it turned to a slushy in the beaker and in the filter as I was filtering the combined filter extractions....
 

slepyyz

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Hey guys, i have bought these:


Can i extract pseudoephedrine from them and if yes how?
 

zaners

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Hey guys, i have bought these:


Can i extract pseudoephedrine from them and if yes how?
slepyyzHave you searched the forum..I'm pretty sure I've seen someone with a extraction with the same ingredients of these pills
 

zaners

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Have you searched the forum..I'm pretty sure I've seen someone with a extraction with the same ingredients of these pills
zaners
 

slepyyz

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zanersThank you. U guys are legends!
 

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Hey guys, i have bought these:


Can i extract pseudoephedrine from them and if yes how?
slepyyzSo you have ibuprofen and pseudo HCl in your pills. Also, whatever the inactive ingredients are, but it's not so important. Pseudoephedrine is not very soluable in acetone.
Ibuprofen is soluable in acetone. Most likely, so is the coating on the pills, and perhaps (hopefully) some of the inactive ingredients. So if there is a color coating, wash it off with cold dry acetone. After you get it off, then crush the pills and dissolve everything into cold dry acetone again. Keep the solids, this is your PSE, get rid of the liquid. Repeat this atleast 3 times. Try to only use just enough acetone to do the job and no extra. Make sure it is cold as you can get it and dry with a dessicant (Mg2SO4) - No moisture! Otherwise you are just wasting your PSE.

After you washed with acetone and you have your solids, now dissolve the solids in dry methanol. PSE is very soluable in methanol. Ibuprofen and the color coating is also, but we got rid of them with the acetone already. So the only other thing with our PSE in the methanol is whatever inactive ingredients that are soluable in methanol that the acetone didn't wash away. If you are doing a SNB, these trace inactives probably won't matter because the SNB reaction is 'dry' - there is little to no H2O, however, if you are doing a RP cook, you may want to check your inactive ingredients and their soluability properties and try to remove them if you need to. You will want to perform this BEFORE you dissolve your solids in methanol. If the only ingredient left with your solids that is soluable in methanol is your PSE, then you don't need to worry. Pour your methanol in an evaporation dish and let it evaporate. Wash your solids with methanol atleast 3 times, filter it very well and combine all of the methanol and let it evaporate. It will crystalize in your dish and you can scrape up some pretty decent grade PSE for experimentation. You should be good to go forward with your PSE at this point.

Good luck, take care.
 

slepyyz

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So you have ibuprofen and pseudo HCl in your pills. Also, whatever the inactive ingredients are, but it's not so important. Pseudoephedrine is not very soluable in acetone.
Ibuprofen is soluable in acetone. Most likely, so is the coating on the pills, and perhaps (hopefully) some of the inactive ingredients. So if there is a color coating, wash it off with cold dry acetone. After you get it off, then crush the pills and dissolve everything into cold dry acetone again. Keep the solids, this is your PSE, get rid of the liquid. Repeat this atleast 3 times. Try to only use just enough acetone to do the job and no extra. Make sure it is cold as you can get it and dry with a dessicant (Mg2SO4) - No moisture! Otherwise you are just wasting your PSE.

After you washed with acetone and you have your solids, now dissolve the solids in dry methanol. PSE is very soluable in methanol. Ibuprofen and the color coating is also, but we got rid of them with the acetone already. So the only other thing with our PSE in the methanol is whatever inactive ingredients that are soluable in methanol that the acetone didn't wash away. If you are doing a SNB, these trace inactives probably won't matter because the SNB reaction is 'dry' - there is little to no H2O, however, if you are doing a RP cook, you may want to check your inactive ingredients and their soluability properties and try to remove them if you need to. You will want to perform this BEFORE you dissolve your solids in methanol. If the only ingredient left with your solids that is soluable in methanol is your PSE, then you don't need to worry. Pour your methanol in an evaporation dish and let it evaporate. Wash your solids with methanol atleast 3 times, filter it very well and combine all of the methanol and let it evaporate. It will crystalize in your dish and you can scrape up some pretty decent grade PSE for experimentation. You should be good to go forward with your PSE at this point.

Good luck, take care.
SoldadoDeDrogasThanks man. U are a legend!
 
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