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William D.

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Jb5UHtnjL6

Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets.
Pseudoephedrine was extracted from Sudafed tablets using ethanol, ethanol/methanol (90:10% vol/vol) and methylated spirits. The solvents were chosen with reference to the relevant clandestine literature. For each extraction, one Sudafed tablet was crushed using a mortar and pestle and placed in a beaker. The iron oxide coating was removed by repetitive washing with acetone (10 mL in total) until all of the red colour had disappeared. The acetone was removed by filtration and the residue was allowed to dry. The extracting solvent (15 mL) was added to the beaker, which was then covered with aluminum foil and the sample shaken using mechanical agitation for 15 min. The sample was left to settle for one hour at room temperature, and then filtered using gravity filtration. The solvent was evaporated, and the resultant solid collected.
>>>>>>>>Other methods are here<<<<<<<<

Iodine from iodine tinctures.
Iodine tincture (7 mL, 2.5%) and distilled water (7 mL) were combined together and mixed with swirling. Concentrated hydrochloric acid (1 mL) was added dropwise with swirling, followed by hydrogen peroxide (7 mL, 6 % 20 vols). The mixture was poured into a beaker containing distilled water (50 mL) and left to stand for 20 min. The mixture was subsequently filtered using gravity filtration to reveal the iodine crystals.

Extraction of red phosphorous from matchboxes.
Matchbook strikers were cut off from locally purchased KTWO safety matchboxes and soaked in acetone (10 mL). After 30 min, the red phosphorous was scrapped from the strikers, and the paper discarded. The extracted red phosphorous was washed with distilled water and left to dry to a constant weight. The dry red phosphorous was placed in a beaker, and sodium hydroxide solution (20% wt/vol, 20 mL) was added. This solution was placed on a low heat for 2 h. The final product was filtered, washed with distilled water and left to dry to a constant weight.

Synthesis of methylamphetamine using the Moscow and Hypophosphorous routes.
Six batches of methylamphetamine hydrochloride were prepared using each synthetic route for laboratory grade pseudoephedrine and pseudoephedrine extracted from Sudafed tablets as previously described. In the case of the extracted precursor samples, the essential chemicals (iodine and phosphorous), used in the synthesis, were also extracted from tinctures and matchboxes. Twenty-four batches of methylamphetamine hydrochloride were prepared using each route, providing 48 batches in total.
GXE3aom9cN

[1] Moscow route:
Pseudoephedrine hydrochloride (2.0 g) was mixed in a round bottom flask (100 mL) together with red phosphorous (0.6 g), iodine (4.0 g) and distilled water (2 mL) and a condenser attached. The mixture was refluxed for 24 h and then allowed to cool. Once cool, the mixture was diluted with an equal volume of water and the red phosphorus filtered out. A few grams of sodium thiosulfate were placed into a beaker, and sodium hydroxide solution (25% wt/vol, 8 mL) added to basify the solution. This was then added to the filtered reaction mixture, and swirled to reveal methylamphetamine free base
As an oil, which floated to the top of the aqueous solution. Toluene (20 mL) was added to extract the methylamphetamine free base. The toluene extract was clear to pale yellow. Anhydrous hydrogen chloride gas was bubbled through to reveal a white precipitate, which was washed with toluene. The solid was dried under high vacuum.

Download Video

[2] Hypophosphorous route:
Pseudoephedrine hydrochloride (2.0 g) was placed into a round bottom flask (100 mL) and mixed with iodine (4.0 g) and hypophosphorous acid (3.6 mL) and a condenser attached. The mixture was refluxed for 8 h, then allowed to cool. Once cool, the mixture was diluted with an equal volume of water. A few grams of sodium thiosulfate were placed into a beaker, and 25 % sodium hydroxide solution (24 mL) was added to extract the methylamphetamine free base. Extraction and precipitation of the salt was as previously described.
 
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ifreezeu

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Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets.

Pseudoephedrine was extracted from Sudafed tablets using ethanol, ethanol/methanol (90:10 % vol/vol) and methylated spirits. The solvents were chosen with reference to the relevant clandestine literature. For each extraction, one Sudafed tablet was crushed using a mortar and pestle and placed in a beaker. The iron oxide coating was removed by repetitive washing with acetone (10 mL in total) until all of the red colour had disappeared. The acetone was removed by filtration and the residue was allowed to dry. The extracting solvent (15 mL) was added to the beaker, which was then covered with aluminum foil and the sample shaken using mechanical agitation for 15 min. The sample was left to settle for one hour at room temperature, and then filtered using gravity filtration. The solvent was evaporated, and the resultant solid collected.


Iodine from iodine tinctures.

Iodine tincture (7 mL, 2.5 %) and distilled water (7 mL) were combined together and mixed with swirling. Concentrated hydrochloric acid (1 mL) was added dropwise with swirling, followed by hydrogen peroxide (7 mL, 6 %20 vols). The mixture was poured into a beaker containing distilled water (50 mL) and left to stand for 20 min. The mixture was subsequently filtered using gravity filtration to reveal the iodine crystals.


Extraction of red phosphorous from matchboxes.

Matchbook strikers were cut off from locally purchased KTWO safety matchboxes and soaked in acetone (10 mL). After 30 min, the red phosphorous was scrapped from the strikers, and the paper discarded. The extracted red phosphorous was washed with distilled water and left to dry to a constant weight. The dry red phosphorous was placed in a beaker, and sodium hydroxide solution (20 % wt/vol, 20 mL) was added. This solution was placed on a low heat for 2 h. The final product was filtered, washed with distilled water and left to dry to a constant weight.


Synthesis of methylamphetamine using the Moscow and Hypophosphorous routes.

Six batches of methylamphetamine hydrochloride were prepared using each synthetic route for laboratory grade pseudoephedrine and pseudoephedrine extracted from Sudafed tablets as previously described. In the case of the extracted precursor samples, the essential chemicals (iodine and phosphorous), used in the synthesis, were also extracted from tinctures and matchboxes. Twenty-four batches of methylamphetamine hydrochloride were prepared using each route, providing 48 batches in total.


Moscow route:

Pseudoephedrine hydrochloride (2.0 g) was mixed in a round bottom flask (100 mL) together with red phosphorous (0.6 g), iodine (4.0 g) and distilled water (2 mL) and a condenser attached. The mixture was refluxed for 24 h and then allowed to cool. Once cool, the mixture was diluted with an equal volume of water and the red phosphorus filtered out. A few grams of sodium thiosulfate were placed into a beaker, and sodium hydroxide solution (25 % wt/vol, 8 mL) added to basify the solution. This was then added to the filtered reaction mixture, and swirled to reveal methylamphetamine free base
As an oil, which floated to the top of the aqueous solution. Toluene (20 mL) was added to extract the methylamphetamine free base. The toluene extract was clear to pale yellow. Anhydrous hydrogen chloride gas was bubbled through to reveal a white precipitate, which was washed with toluene. The solid was dried under high vacuum.


Hypophosphorous route:

Pseudoephedrine hydrochloride (2.0 g) was placed into a round bottom flask (100 mL) and mixed with iodine (4.0 g) and hypophosphorous acid (3.6 mL) and a condenser attached. The mixture was refluxed for 8 h then allowed to cool. Once cool, the mixture was diluted with an equal volume of water. A few grams of sodium thiosulfate were placed into a beaker, and 25 % sodium hydroxide solution (24 mL) was added to extract the methylamphetamine free base. Extraction and precipitation of the salt was as previously described.
William Dampier
Hi

I have just ordered these.


Or shall I order these, if they will be easier to work with ?


Ingredients below.

Ephedrine 30mg
Caffeine 200mg
Aspirin 30mg


1. How can I remove Aspirin out of this using the most simplest of the methods ?
(Aspirin is not water soluble but ephedrine is soluble ? Can I take that route ? Grind pills add to water then gravity filter (Aspirin remains on the filter) I get the Epherdrine + Caffeine + Water)
Hmm how do I remove the solubles (Ephedrine + Caffeine) from the water ?

2. How can I extract only ephedrine out of the tablets using the most simplest of the methods, if any ?

Thanks in Advance
 
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G.Patton

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Hi

I have just ordered these.


Or shall I order these, if they will be easier to work with ?


Ingredients below.

Ephedrine 30mg
Caffeine 200mg
Aspirin 30mg


1. How can I remove Aspirin out of this using the most simplest of the methods ?
(Aspirin is not water soluble but ephedrine is soluble ? Can I take that route ? Grind pills add to water then gravity filter (Aspirin remains on the filter) I get the Epherdrine + Caffeine + Water)
Hmm how do I remove the solubles (Ephedrine + Caffeine) from the water ?

2. How can I extract only ephedrine out of the tablets using the most simplest of the methods, if any ?

Thanks in Advance
ifreezeuAspirin 10 g/100 ml ethyl ether
Caffeine 0.2 g/100 ml ethyl ether
Ephedrine insoluble in ether
Use anhydrous ether!
 

Joeking

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Aspirin 10 g/100 ml ethyl ether
Caffeine 0.2 g/100 ml ethyl ether
Ephedrine insoluble in ether
Use anhydrous ether!
G.PattonHi legend, I can't for the life of me figure out how to seperate the ephedrine from the caffeine as they are both insoluble in ethyl ether, do you have any idea, TIA.
 

pdwshopnl

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How Look situaction with CIRRUS tabletts in EU?
I hear first step is remove shell from all tablets - hands - (more time process) in acetone, next if are dry grinding for powder, next extraction with toluene 2-3x (in toluene is of course unwanted product stopped reaction becouse hydrochloride dont disolve in toluen)- filtrate and this extract out.
Next filtrate alkalise IT for change pseudoephedrine hydrochloride to base and extraction one again (3 times minimum) with ether/toluene/etc and gassing hcl to neutral ph and for end filtrate, dryiness to get pseudoephedrine hcl ready to Next step
 

William D.

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What Cirrus contains
• Active ingredients:
Each tablet contains 5 mg cetirizine dihydrochloride in an immediate release form
and 120 mg pseudoephedrine hydrochloride in a prolonged-release form.
• Other non-active ingredients:
Hypromellose.
Microcrystalline cellulose.
Colloidal silica anhydrous.
Magnesium stearate.
Lactose monohydrate

pdwshopnl, in general, your route of extraction looks good. Prolonged-release form - and there is a shell of tablets. Before extraction of toluene, it is necessary to dissolve everything in warm water, filter from insoluble and after already extracted with toluene.
 
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primitiveintelectual

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Moscow route and Hypophosphorous route: how does the reaction work? so what temperatures need to be maintained from start to finish?
Moscow route: 24h Reflux must be or may be less?
 

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Temperatures are brought to a boil, the exact time of reaction is only by TLC
 

Tincan88

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Temperatures are brought to a boil, the exact time of reaction is only by TLC
William DampierSince your en expert is the shit coming from Mexico meth. And is all meth just say we had shit from moscow route birch reduction and any other route you can think of . Would it all be the Same . Keep you high for awhile. Cuz this shit know gets you high for a few hours and so I’m thinking is it even meth
 

primitiveintelectual

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TLC? what is it?
 

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primitiveintelectualTLC = Tender Loving Care
Meaning temp is adjusted until a good reflux is achieved (reflux ring in the lower 1/3 of the condenser).
Time will vary as well, but 24 hours is a good starting point for a first time. Observations of changes to the reflux will show when it is finished
 

yuiopjkl

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How much methamphetamine can 100 grams of pseudoephedrine pills make?
 

Tincan88

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How much methamphetamine can 100 grams of pseudoephedrine pills make?
yuiopjklWas it pulled out of pills or befor it was put in and if so what is the going rate on pseudo Can you get pharmaceutical grade pseudo of a market place? Cuz you can only buy like 9 grams a month where I’m at and iv have to put people in my biz to get any thing worth wild.
 
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brianvene1

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A few grams of sodium thiosulfate were placed into a beaker, and 25 % sodium hydroxide solution (24 mL) was added to extract the methylamphetamine free base. Extraction and precipitation of the salt was as previously described.
William DampierW.D, G.P
1-Can i use the toluene extraction after Hypophosphorous refluxe?
2-What is the purity obtained, and how to improve it?
3-What is the maximum amount that can be synthesized with these methods?

thank you
 

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1-Can i use the toluene extraction after Hypophosphorous refluxe?
2-What is the purity obtained, and how to improve it?
3-What is the maximum amount that can be synthesized with these methods?
brianvene1u use this synthesis (click). In the end, we add an aqueous alkali solution to the basic pH (>10). Toluene can be used for extraction. Extract we can wash with water, brine, thiosulfate (to wash the remaining iodine). The reaction is well scaled if there is a necessary equipment (good stirring, sufficient volume of a flasks and controlled reflux). But scaling must be made gradually (if there is no experience)
 
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ice

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u use this synthesis (click). In the end, we add an aqueous alkali solution to the basic pH (>10). Toluene can be used for extraction. Extract we can wash with water, brine, thiosulfate (to wash the remaining iodine). The reaction is well scaled if there is a necessary equipment (good stirring, sufficient volume of a flasks and controlled reflux). But scaling must be made gradually (if there is no experience)
William DampierHello, I follow the Moscow route. In the last step, hydrogen chloride gas is passed into the toluene extraction solution, and some transparent crystalline substances are obtained in the wall of the beaker, unlike the white powder in the video. I simply can't stand the pungent smell of hydrogen chloride gas. When the toluene solution is poured out at the end, there is still a small amount of yellow oily liquid at the bottom of the beaker. Am I not introducing enough hydrogen chloride?
 

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ralralro

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To do this, what materials and equipment do you recommend?
 

ralralro

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How to make 25% Sodium Hydroxide with 5% Sodium Hydroxide?
Can epadrine be used instead of pseudoephedrine?
 
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ralralro

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I have a lot of questions, so I've put them together and
don't know how to delete the above question, so I'm re-registering

1. How to dry under high vacuum
2. How to Extract Hypophosphorous Acid with Sodium Hypochlorite
3. What equipment do you use for extraction with toluene?
4. Can epadrine be used instead of pseudoephedrine?
5. How to make 25% Sodium Hydroxide with 5% Sodium Hydroxide?
6. How much grams of sodium thiosulfate do i have to use with Hypophosphorous route

I'm a beginner so I have a lot of questions, sorry and thank you for your help
 

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Since the Moscow route seems to differ from the usual HI/RP method only in that it simply uses I2 in place of HI, my question is -- why don't people use the Moscow route more often? Are yields generally similar to the HI method? What's the catch? Great write-up btw
 
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