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Instructions, videos, tutorials, reviews of experimental synthesis, distillation and recrystallization of chemicals.
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Synthesis of Amphetamines (Phenylethylamines)
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Methylamine HCl synthesis
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https://bbgate.com/threads/methylamine-hydrochloride-synthesis-large-scale.617/
NileRed video
https://www.youtube.com/watch?v=wuyouolU5LY
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methylamine
methylamine hcl synthesis
Sodium acetate (NaOAc) synthesis
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https://bbgate.com/threads/acetic-anhydride-syntheses.648/
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acetic anhydride synthesis
A Simple Distillation manual
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https://bbgate.com/threads/distillation-and-distillation-systems.485/
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Separating Liquids by Distillation
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https://bbgate.com/threads/distillation-and-distillation-systems.485/
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Vacuum desiccator manual
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https://bbgate.com/threads/vacuum-desiccators.532/
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Magnetic stirrer manual
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https://bbgate.com/threads/magnetic-stirrer.524/
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Rotary evaporator (How to use a Rotavap)
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https://bbgate.com/threads/rotary-evaporator-and-additional-equipment.478/
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Preparation of hydrogen gas
Laboratory FAQ
https://bbgate.com/threads/hydrogen-gas-h2-laboratory-preparation.1013/
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Hydrogenation in small scale with Pd/C catalyst
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https://bbgate.com/threads/hydrogen-gas-h2-laboratory-preparation.1013/
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hydrogenation in small scale with pd/c catalyst
Making a Dry Ice Acetone bath
Laboratory FAQ
http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/threads/dry-ice-78-5-deg-laboratory-handling.1331/
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Liquid nitrogen (N2) bath handling
Laboratory FAQ
http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/threads/liquid-nitrogen-n2-laboratory-handling.1362/
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liquid nitrogen (n2) bath handling
Aluminium amalgam (Al/Hg) synthesis
Laboratory FAQ
https://bbgate.com/threads/aluminium-amalgam-al-hg-summary.1271/
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Mercury Nitrate and Aluminium Amalgam Synthesis
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https://bbgate.com/threads/aluminium-amalgam-al-hg-summary.1271/
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Amphetamine synthesis from P2NP via Al/Hg (video)
Synthesis of Amphetamines (Phenylethylamines)
https://bbgate.com/threads/synthesis-of-amphetamine-from-p2np-via-al-hg-video.196/
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Acid-Base Extraction
Laboratory FAQ
http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/threads/extraction.553/
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Liquid-Liquid Extraction
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http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/threads/extraction.553/
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The single punch tablet press
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http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/threads/tableting.348/
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Dimethylamine synthesis from N,N-dimethylformamide
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Dimethylamine synthesis from N,N-dimethylformamide
https://www.youtube.com/watch?v=D1pvqXeh3TE
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Acetic anhydride synthesis
Other Video Tutorials
Acetic anhydride synthesis tutorial post:
https://bbgate.com/threads/acetic-anhydride-syntheses.648/
Thy Labs video
https://www.youtube.com/watch?v=xpuUn5bZxzY
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MDA Synthesis. Part 1 of 3.
MDA Synthesis. Part 2 of 3.
MDA Hydrochloride Synthesis From Amine. Part 3 of 3.
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